Comparison between fluctuation of floating potential gradient and velocity of blob structure on HL-2A tokamak

Several results based on the Langmuir probes' data on the HL-2A tokamak are presented. The blob structures' radial and poloidal drift velocities, estimated by the gradient of floating potential and by time delay evaluation, are compared in different line-averaged density and electron cyclotron resonance heating conditions. A positive correlation is observed in the comparison between blobs' radial velocity estimated by the two methods mentioned above, regardless of the situation differences mentioned above. Correlation is also observed in the comparison between the blobs' poloidal velocity estimated by the two methods in different situations, while a shift due to the different line-averaged density is observed. These results imply that the radial gradient of floating potential may have some value as a reference during data analysis in low-parameter discharge.     

核磁共振波谱法测定臭氧化橄榄油中的活性成分含量

以橄榄油为原料,经臭氧氧化制备臭氧化橄榄油。利用核磁共振(NMR)采集碳谱数据,积分碳谱特征峰,计算橄榄油被氧化成分的相对含量。结果表明:臭氧化橄榄油与橄榄油碳谱有明显的区别,臭氧化橄榄油在δ103.1处出现新峰,对应δ130.1处的峰高减弱,这是由于橄榄油中的不饱和双键被氧化。采用该方法测得5个臭氧化油中活性成分含量分别为21.46%、21.03%、21.31%、18.71%和24.42%。采用核磁共振波谱法测定臭氧化橄榄油的活性成分含量具有操作简单,不需要预处理,结果可靠的优点。     

电动汽车用动力电池振动疲劳测试方法开发

动力电池是当前新能源汽车中的核心零件,其性能,安全,可靠与耐久性直接影响整个车辆安全耐久性能,而电池系统的抗振动冲击特性是产品开发设计过程中需要满足的重要指标.文中着重阐述动力电池振动疲劳的测试验证策略与具体实施指导,为电池系统研发和测试工作提供重要参考.     

基于SMA驱动的连续体手术机器人研究综述

连续体机器人是一种能在工作空间中连续弯曲的机器人,因其能在非结构化和狭窄的环境中灵活运动而得到广泛的关注.形状记忆合金(Shape memory alloy,SMA)材料具有良好的形状记忆效应和超弹性,通过施加不同的温度便能够实现对SMA的形状控制,是作为连续体机器人驱动装置的理想材料.基于SMA驱动的连续体机器人有着结构体积小,控制简便,运动范围广,自由度高,易于避障等优点,十分适用于环境复杂的医疗手术环境之中.对SMA的驱动原理和方式进行了分析,介绍了基于SMA驱动的连续体机器入在医疗手术方面的研究现状及建模方法,最后,对发展趋势进行了展望.     

地铁车辆空气制动管路保压试验的改进方案

分析了地铁车辆空气制动管路组装完毕后的保压试验操作过程,识别了其中的问题项点,提出了有针对性的优化改进方案,使保压试验结果准确可靠.     

生物矿化法制备氧化镓颗粒及其性能表征

以蚕丝蛋白为模板,在相对温和的条件下通过生物矿化的手段形成具有特殊形貌的α-GaOOH颗粒,并通过在不同温度下煅烧α-GaOOH得到α-Ga2O3和β-Ga2O3.采用扫描电镜(SEM)、透射电镜(TEM)、X射线衍射仪(XRD)和荧光分光光度计(PL)等手段研究了丝素蛋白多肽和矿化时间对颗粒的影响,对其生物矿化机理进行了初步探讨.结果表明,所制备的β-Ga2O3具有优良的发光特性,丝素蛋白多肽模板以无定形的结构与产物结合在一起,并且经过高温烧结后仍以碳膜的形式包覆在材料的表面.这种碳膜结构对于提高材料的生物学性能起着重要的作用.     

Lithiation MXene Derivative Skeletons for Wide-Temperature Lithium Metal Anodes

Lithium (Li) metal, as an appealing candidate for the next-generation of high-energy-density batteries, is plagued by its safety issue mainly caused by uncontrolled dendrite growth and infinite volume expansion. Developing new materials that can improve the performance of Li-metal anode is one of the urgent tasks. Herein, a new MXene derivative containing pure rutile TiO₂ and N-doped carbon prepared by heat-treating MXene under a mixing gas, exhibiting high chemical activity in molten Li, is reported. The lithiation MXene derivative with a hybrid of LiTiO₂-Li₃N-C and Li offers outstanding electrochemical properties. The symmetrical cell assembling lithiation MXene derivative hybrid anode exhibits an ultra-long cycle lifespan of 2000 h with an overpotential of ≈30 mV at 1 mA cm⁻², which overwhelms Li-based anodes reported so far. Additionally, long-term operations of 34, 350, and 500 h at 10 mA cm⁻² can be achieved in symmetrical cells at temperatures of −10, 25, and 50 °C, respectively. Both experimental tests and density functional theory calculations confirm that the LiTiO₂-Li₃N-C skeleton serves as a promising host for Li infusion by alleviating volume variation. Simultaneously, the superlithiophilic interphase of Li₃N guides Li deposition along the LiTiO₂-Li₃N-C skeleton to avoid dendrite growth.     

响应曲面法优化衣康酸三元共聚物制备工艺

针对咸阳某企业循环冷却水水质情况,选择衣康酸(IA)、乙酸乙烯酯(VAc)和2-丙烯酰胺-2-甲基丙磺酸(AMPS)为单体,采用水溶液自由基聚合法制备IA-VAc-AMPS共聚物阻垢剂.利用响应曲面Box-Behnken试验优化共聚物制备工艺,并建立多元回归模型.结果表明:单体摩尔比和反应温度影响最大,单体摩尔比和引发剂用量交互影响最为显著;响应曲面确定的最优合成条件为:单体摩尔比1.36、引发剂7.11％、反应温度82.73℃和反应时间2.87 h,最优条件下合成共聚物的阻垢率达到97.56％.FT-IR光谱表征表明已成功制备IA-VAc-AMPS三元共聚物.SEM对垢样晶体形态结构分析表明共聚物作用效果明显,垢体松散,致密度降低.     

农药沉积利用率喷雾指示剂诱惑红的酶标仪测定方法

诱惑红是一种水溶性染料,近年来被用作农药沉积利用率测定的指示剂。诱惑红的检测方法为高效液相色谱法和分光光度法。高效液相色谱法需要专门的分析仪器,且价格昂贵,可见分光光度计法操作繁琐,试剂用量大,耗时长,均不适宜田间快速高效测定。笔者发展了诱惑红的酶标仪测定方法,简单高效,可批量检测多个样品,且准确度和精密度高,线性关系良好,514 nm检测波长下不受其他农药影响,并应用于玉米无人飞机喷雾场景下农药雾滴在玉米冠层的沉积利用率测定。